Pseudoephedrine AcetateJust a repri

Pseudoephedrine Acetate

Just a reprint. What do I think? Well, I would like the titled material to be analogous to chloroephedrine, but this is just a salt of the amine using acetic as the acid, a result of the isolation process from pills. Much of it is in traffic in Mexico; apparently the superlabs also purchase material which at one time was in pills. The second article is about a seizure.

Meth Synthesis W/ephedrine, HI, Red Phosphorus
by Cousin Singe
NOTICE: TO ALL CONCERNED Certain text files and messages contained on this site deal with activities and devices which would be in violation of various Federal, State, and local laws if actually carried out or constructed. The webmasters of this site do not advocate the breaking of any law. Our text files and message bases are for informational purposes only. We recommend that you contact your local law enforcement officials before undertaking any project based upon any information obtained from this or any other web site. We do not guarantee that any of the information contained on this system is correct, workable, or factual. We are not responsible for, nor do we assume any liability for, damages resulting from the use of any information on this site.

All you people who want an easy meth systhesis – They don’t exist! You have to know some chemistry. Learn some (yes it takes some discipline) or be doomed to fail.

So, again, this information is posted for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and/or imprisonment. If you are stupid enough to actually manufacture meth you WILL probably go to prison. This is the 90's.

So to make meth from ephedrine- Using l- or pseudo ephedrine place 1000 gms of ephedrine, 250gms of red phosphorus, and 1000ml of hydriotic acid in a suitable round bottom flask. Fit the flask with a reflux condenser and reflux the mixture for 48hrs at 120 degrees C. Add a 10% solution of sodium hydroxide until the Ph is 14. You should get an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a flask with 3 volumes of water. Rig the flask for distillation and distill the oil water mixture until the oil is mostly gone (except for highly colored globs of oil.) In the reciever flask there should be two layers, an upper oil layer and a lower water layer. Separate the oil layer and mix it with 10% hydrochloric acid until the Ph is 7.6. evaporate the water and it will crystallize into methamphetamine hcl.

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“We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. Ephedrine was reacted with red phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and iodine; when red phosphorus and iodine are in excess of ephedrine in a 1:3.8:7.2 molar ratio (ephedrine:red phosphorus:iodine) methamphetamine is formed and the ephedrine is consumed in 8 hours.”

Anyone have any thoughts, experience with the typical E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. It seems like that is what is being described (along with acid substitution).

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Materials:

1. 30ml bottle tincture iodine containing 2% iodine, sodium iodide 2.4%, alcohol 47%, rest H20

2. 5 Sinustop Herbal Decongestant tablets containing 60mg crystaline pseudoephedrine HCl each mixed with some herbal ingrediants. Or 300mg of ephedrine obtained thru some other method.

3. 5 road flares.

4. Bottle of drain cleaner containg conc. H2SO4

5. Bottle white distilled vinegar

6. Red devil Lye containing sodium hydroxide

7. Spray can of brake cleaner containing 1,1,1 trichloroethylene or 1,1,1 trichloroethane

Procedure:

A. Purifying pseudoephedrine:

1. Take the 5 decongestant capsules, empty their contents into a small funnel with a coffee filter. Pour 50ml of cold water through the filter, and collect the liquid in a small jar.

2. Add a 1/4tsp of lye to the collected liquid. You should immediately smell the odor of ephedrine.

3. Put the resultant solution in another small jar, and add 50ml of brake cleaner, then close the lid and shake vigorously. Let stand so that the layers seperate.

4. Using a turkey baster, suck up the bottom brake cleaner layer out of the jar and put it into a small bowl.

5. Add 50ml of vinegar and heat the resultant mixure over low heat in a frying pan with 1/2 inch of water. Thus a water bath. Do not use a gas stove, since the brake cleaner vapors will produce toxic phosgene if there is contact with a flame. Instead use a hot plate or electric stove at low heat only.

6. Heat the bowl in the water bath until no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine acetate.

B. Preparing the red phosphorus:

1. Scrape the red phosphorus off of the caps of the 5 flares and store for later use. You should get about 0.1g per flare.

C. Preparing the iodine/HI solution:

1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.

D. The reaction:

1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.

E: Extraction:

1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.

Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)

Best regards, Cousin Singe

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FAQ fodder…

If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.

The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.

When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.

[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]

Kết quả (Ả Rập) 3:

Pseudoephedrine بشكلJust a reprint. What do I think؟ حسنا, I would like the titled material to be analogous to تعتبر مواد الكلوروإيفيدرين والميثيل, but this is just a salt of the أمين using acetic as the acid, a result of the isolation process from تلك....... Much of it is in the traffic in Mexico؛ على superlabs also purchase material which at one time was in تلك. The second article is about أ - متأخر -ميث Synthesis ث / ephedrine، مرحبا، Phosphorus Redعم Singe byNOTICE: إلى جميع CONCERNED files and Certain text messages contained on this site deal with which would be in activities and devices violation of various Federal, State, and local laws if actually carried out or constructed. The webmasters of this site do not advocate of any breaking the law - Our النص files and message bases for informational purposes are فقط....... We recommend that you local law enforcement officials before contact your undertaking any project based upon any information obtained from this or any other web site. We do not guarantee that any of the information contained on this system is الصحيح، workable, or are not responsible for factual. We do we assume, nor any liability for، damages resulting from the use of any informationon this site.All you people who want an سهلة meth systhesis – They لا exist. You have to know some chemistry. Learn some (نعم it takes some الانضباط or be doomed to fail.So this information is posted، مرة أخرى، for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and / or imprisonment. If you are غبي enough to actually manufacture meth you will go to prison. This is probably the 90 's.So to make meth from ephedrine - Using ل or الأولى ephedrine place of ephedrine 1000 جم، 250gms of red phosphorus and 1000 of hydriotic acid in a مناسبة جولة أسفل القارورة - صالح the قارورة with a reflux reflux condenser and the mixture for 48hrs at 120 درجة جيم - إضافة 10% solution of sodium hydroxide until the Ph 14 - You should get is an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a قارورة with 3 volumes of water. لديك قارورة distillation and for the distill the oil water mixture until the oil is mostly ذهب (except for highly الملونة globs of oil). In the reciever قارورة there should be two الطبقات، an upper oil layer and a lower water layer. Separate and it with the oil طبقة مزيج hydrochloric 10%حمض until the Ph is 7-6. evaporate the water and it will crystallize into إن حمض الهيدروكلوريك.--"We have observed that phosphorus and mixtures containing الأحمر، iodine either concentrated حمض الهيدروكلوريك or glacial acetic acid do to إن تحويل ephedrine; however, when the phosphorus is omitted، إن is not formed....... Ephedrine was reacted with الأحمر phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and when الأحمر phosphorus and iodine iodine؛ are in الزائدة of ephedrine in a 1: 3-8: 7-2 molar ratio (ephedrine: الأحمر phosphorus: iodine) إن is formed and the ephedrine is consumed in 8 ساعات".علينا have any thoughts، experience with the الجسم E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. يبدو like that is what is being described (along with acid substitution).--Materials:1 - 30ml زجاجة tincture iodine containing 2% iodine. iodide 2.4 في المائة، الكحول 47 ٪، والباقي H202 - 5 Sinustop Herbal Decongestant tablets containing 60 ملغ crystaline pseudoephedrine حمض الهيدروكلوريك each مختلطة with some herbal ingrediants - أو 300 ملغ of ephedrine obtained thru some other method.3 - 5 flares road.4 - زجاجة of drain cleaner containg H2SO4 conc.5 - زجاجة بيضاء distilled بعض6 - Red الشيطان الغسول containing sodium hydroxide7 - رذاذ can of 198KB cleaner containing 1, 1, 1 trichloroethylene or 1, 1, 1 trichloroethaneالداخلي:ألف - Purifying pseudoephedrine:1 - Take the 5 decongestant كبسولات، فارغة their contents into a small funnel with a القهوة filter. Pour 50 مل of الباردة water through the فلتر, and collect the liquid in a small جرة.2 - إضافة 1 / 4tsp of lye to the collected السائل - You should immediately غوين the odor of ephedrine.3 - وضع the resultant solution in another and small جرة، إضافة 50 مل of 198KB آن، ثم close the غطاء and يا vigorously - Let stand so that the seperate layers.4 - Using a تركيا baster تمتص up the bottom الفرامل، آن layer out of the جرة and put it into a small وعاء.5 - إضافة 50 مل of and the resultant بعض الحرارة حرارة mixure over low in a frying بان with 1 / 2 بوصة of water....... وهكذا....... Do not use حمام a water gas ليس أ، since the cleaner 198KB vapors will produce toxic phosgene if there is contact with a flame - Instead use or at لوحة الساخنة الكهربائية ليس أ انخفاض الحرارة only.6 - الحرارة وعاء in the water until the حمام no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine خلات.باء - Prepari