Pseudoephedrine AcetateJust a repri

Pseudoephedrine Acetate

Just a reprint. What do I think? Well, I would like the titled material to be analogous to chloroephedrine, but this is just a salt of the amine using acetic as the acid, a result of the isolation process from pills. Much of it is in traffic in Mexico; apparently the superlabs also purchase material which at one time was in pills. The second article is about a seizure.

Meth Synthesis W/ephedrine, HI, Red Phosphorus
by Cousin Singe
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All you people who want an easy meth systhesis – They don’t exist! You have to know some chemistry. Learn some (yes it takes some discipline) or be doomed to fail.

So, again, this information is posted for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and/or imprisonment. If you are stupid enough to actually manufacture meth you WILL probably go to prison. This is the 90's.

So to make meth from ephedrine- Using l- or pseudo ephedrine place 1000 gms of ephedrine, 250gms of red phosphorus, and 1000ml of hydriotic acid in a suitable round bottom flask. Fit the flask with a reflux condenser and reflux the mixture for 48hrs at 120 degrees C. Add a 10% solution of sodium hydroxide until the Ph is 14. You should get an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a flask with 3 volumes of water. Rig the flask for distillation and distill the oil water mixture until the oil is mostly gone (except for highly colored globs of oil.) In the reciever flask there should be two layers, an upper oil layer and a lower water layer. Separate the oil layer and mix it with 10% hydrochloric acid until the Ph is 7.6. evaporate the water and it will crystallize into methamphetamine hcl.

——

“We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. Ephedrine was reacted with red phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and iodine; when red phosphorus and iodine are in excess of ephedrine in a 1:3.8:7.2 molar ratio (ephedrine:red phosphorus:iodine) methamphetamine is formed and the ephedrine is consumed in 8 hours.”

Anyone have any thoughts, experience with the typical E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. It seems like that is what is being described (along with acid substitution).

——

Materials:

1. 30ml bottle tincture iodine containing 2% iodine, sodium iodide 2.4%, alcohol 47%, rest H20

2. 5 Sinustop Herbal Decongestant tablets containing 60mg crystaline pseudoephedrine HCl each mixed with some herbal ingrediants. Or 300mg of ephedrine obtained thru some other method.

3. 5 road flares.

4. Bottle of drain cleaner containg conc. H2SO4

5. Bottle white distilled vinegar

6. Red devil Lye containing sodium hydroxide

7. Spray can of brake cleaner containing 1,1,1 trichloroethylene or 1,1,1 trichloroethane

Procedure:

A. Purifying pseudoephedrine:

1. Take the 5 decongestant capsules, empty their contents into a small funnel with a coffee filter. Pour 50ml of cold water through the filter, and collect the liquid in a small jar.

2. Add a 1/4tsp of lye to the collected liquid. You should immediately smell the odor of ephedrine.

3. Put the resultant solution in another small jar, and add 50ml of brake cleaner, then close the lid and shake vigorously. Let stand so that the layers seperate.

4. Using a turkey baster, suck up the bottom brake cleaner layer out of the jar and put it into a small bowl.

5. Add 50ml of vinegar and heat the resultant mixure over low heat in a frying pan with 1/2 inch of water. Thus a water bath. Do not use a gas stove, since the brake cleaner vapors will produce toxic phosgene if there is contact with a flame. Instead use a hot plate or electric stove at low heat only.

6. Heat the bowl in the water bath until no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine acetate.

B. Preparing the red phosphorus:

1. Scrape the red phosphorus off of the caps of the 5 flares and store for later use. You should get about 0.1g per flare.

C. Preparing the iodine/HI solution:

1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.

D. The reaction:

1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.

E: Extraction:

1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.

Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)

Best regards, Cousin Singe

————

FAQ fodder…

If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.

The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.

When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.

[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]

Kết quả (Anh) 3:

复方醋酸只是一个转载。我怎么想？嗯，我想标题的材料是类似于氯麻黄素，但这只是一个盐的胺乙酸的酸，从药隔离过程的结果。它在墨西哥的交通是多；显然superlabs还购买材料，这一次是在丸。二篇文章是关于癫痫发作的。甲基合成W /麻黄素，嗨，红磷表姐单通知：对本网站所包含的某些文本文件和邮件进行处理，如果实际执行或构建的话，将违反联邦、州和地方法律的活动和设备。这个网站的站长不提倡任何触犯法律。我们的文本文件和信息库只用于信息的目的。我们建议您在进行任何项目的基础上与当地执法人员联系，以获得从本网站或其他网站获得的任何信息。我们不能保证本系统所包含的任何信息是正确的、可行的或事实的。我们不承担责任，也不承担任何责任，因使用本网站的任何信息而造成的损害赔偿责任。所有的人谁想要一个简单的方法合成–它们不存在！你必须知道一些化学。学习一些（是的，它需要一些学科）或注定要失败。因此，再次，这个信息是张贴信息的目的。我不承担任何责任，任何人实际上使用这。如果你这样做，你将受到国家和联邦法律，将受到罚款和/或监禁。如果你蠢到实际制作方法你可能会坐牢。这是90年代。所以从麻黄碱制造冰毒使用L或伪麻黄素1000克麻黄碱，红磷250gms，和在一个合适的hydriotic酸1000ml圆底烧瓶。适合瓶与回流冷凝器，回流120摄氏度加氢氧化钠溶液10%为48混合物直到pH为14。你应该得到一个油层和水层。分离油层的分液漏斗，把它与3体积的水瓶。蒸馏烧瓶和蒸馏装置油水混合物直到油大多消失了（除了高色油水珠。）在接收瓶应该有两层，上层油层和下部水层。用10%的盐酸将油层分离，然后用的盐酸混合，直到PH值为7.6。将水蒸发，将结晶成甲基氯化氢。——“我们已经观察到，混合物中含有红色的磷，碘，无论是浓盐酸或冰醋酸做转换成盐酸的甲基安非他明，但是，当磷被省略，甲基安非他明没有形成。麻黄碱对红磷和碘在回流的水，不同的红磷和碘的比率；当红磷和碘在1:3.8:7.2麻黄碱（麻黄素过量摩尔比：红磷：碘）形成甲基安非他明和麻黄素是在8小时内食用。”任何人有任何的想法、经验与典型的e-rp-ha当创建hydriotic酸通常单独的步骤被遗漏的三种化学物质是在回流的水反应。这似乎是正在被描述的（连同酸替代）。——材料：1。30ml瓶碘酒含有2%的碘，碘酸钠2.4%，乙醇47%，其余的水2。5 sinustop中药消肿片含盐酸伪麻黄碱60mg结晶每个混合一些草药成分。或300mg麻黄碱通过其他方法获得。3。5路照明弹。4。含浓缩清洁引流瓶。硫酸5。瓶白蒸馏醋6。红魔鬼碱液含有氢氧化钠7。喷雾可以制动含有1,1,1三氯乙烯或1,1,1三氯乙烷清洁程序：A.净化伪麻黄碱：1。以5减充血剂胶囊，空的内容到一个咖啡过滤漏斗。泼冷水50ml通过过滤器，并在一个小罐子收集液体。2。加1茶匙碱液收集的液体。你应该立即闻到一味的气味。3。将所得溶液在另一个小罐子，加刹车清洁剂50ml，然后盖上盖子，用力摇动。让我们站在这样的层分离。4。用火鸡油、吸底刹车清洁层从罐子里放进一个小碗。5。加入50ml醋，小火加热锅中的水1 / 2英寸所得的混合液。因此，一个水浴。不要使用煤气炉，因为刹车清洁蒸汽都有接触火焰产生有毒的光气。取而代之的是使用热板或电热炉在低热量。6。把碗中的水加热，直到没有更多的液体被留下。在底部会形成一层固体伪麻黄碱醋酸。B.制备